The preparation of anisaldehyde by ozonolysis reaction from anethole was studied.
以茴香脑为原料,乙酸和环己烷的混合物做溶剂,臭氧化法制备茴香醛。
The preparation of anisaldehyde by ozonolysis reaction from anethole was studied.
以茴香脑为原料,乙酸和环己烷的混合物做溶剂,臭氧化法制备茴香醛。
The synthetic method of trichloromethyl-benzyl-alcohol and trichlorometyl-benzyl-alcohol-acetate were reviewed, and the application of rosone were introduced.
讨论
三氯甲基苄醇和三氯甲基苄醇乙酸酯的合成方法,介绍
结晶玫瑰的应
。
The hexadecanol bischloroacetate was synthesized fastly with the technique of microwave irradiation with the anhydrous cupric sulfate as catalyst.


在无水硫酸铜的催化下,利
微波辐射技术快速合成氯乙酸十六酯的方法及影响反应收率的因素。
The stability,decomposition and generation of the acetic acid halid and other organic halide in the treated water is briefly discussed.
简述
成的卤化乙酸和其它有机卤化物的稳定性及分解、
成等问题.
The synthesis of epalrestat,an aldose reductase inhibitor, was improved. The yield of its intermediate 3-carboxymethyl rhodanine was raised to 76.4%.
对醛搪还原酶抑制剂依帕司他的合成工艺作
改
,使中间体绕丹宁乙酸的收率提高到76.4%。
A new method of gas chromatographic analyses in the production of chloroacetic acid for process control using diazomethane as esterification agent is studied.
以重氮甲烷为酯化剂,
气相色谱法对氯乙酸
产的中控分析



。
The present situation of terpinyl acetate synthesis has been reviewed.One-step and two-steps process for the synthesis of terpinyl acetate and relevant reaction mechanism are discussed.
综述
乙酸松油酯的合成
现状,讨论
一步法和两步法合成工艺及相应的反应机理。
When the complex of anhydrous zinc acetate with 1,5-naphthalene diamine was formed, the anhydrous zinc acetate changed from a bidentate ligand to a unidentate ligand.
在无水乙酸锌与1,5-萘二胺形成配位络合物的过程中,无水乙酸锌的结构从双齿型转变成单齿型。
Keto-enol tautomerizing of ethyl acetoacetate was studied by UV.It was conformed that the content of enol ethyl acetoacetate decreased with the increasing polarity of solvents.
本文以紫外光谱为手段
乙酰乙酸乙酯的酮-烯醇式互变异构现象;所得结果证实其烯醇式含量随溶剂极性的增加而减少。
Using sodium hydrosulphide or sodium thiosulfate as materials,the production cost of TGA is low.While,a high content of TGA can be obtained with thiourea as reactant.
本文对巯基乙酸的合成工艺

比较
,认为硫氢化钠法和硫代硫酸钠法
产成本低,适宜于选矿
巯基乙酸的
产,而硫脲法可得到较高浓度的巯基乙酸。
The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.
以异丙醇为溶剂,壬醇为内标,采
气相色谱-质谱法分析
卷烟烟气总粒相物中的游离乙酸,乙酸测定结果的相对标准偏差小于1%,平均回收率为99。
Results indicate that both of barium thioglycolate and barium-natrium thioglycolate can increase the thermal stability of PVC system, and the thermal stability of barium thioglycolate is better.
巯基乙酸钡和巯基乙酸钡-钠都能提高PVC的热稳定性,但巯基乙酸钡的稳定性要好于巯基乙酸钡-钠。
Methyl thioacetate was prepared by using acetyl chloride and methyl mercaptan as starting raw material in this paper.The yield of product is 69.3%.Itcan be used in seasoning flavor.
对可
于各种调味香精的食
香料硫代乙酸甲酯的合成

初步
,产率达到693%,对所合成的产品做
红外光谱分析和质子核磁共振分析,确定
其化学结构。
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